Delta Chemsol
Kandivali, Mumbai, Maharashtra
GST No. 27AMAPM6647F1ZZ
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| Order No | P.O T120150713-CC |
| L/C No | 560Lco1152010006 |
| Commodity | Pentaery thritol |
| Lot No | 150713T |
| Quantity | 20000 Kg |
| Characteristic | Result |
| Purity | 99.00% |
| Hydroxyl content | 48.90% |
| Moisture Content | 0.02% |
| Coloration Degree by phtalic acid resin | 1 |
| Melting point in deg C beginning of melting | Min 180 |
| Appearance | White Powder |
| Prue Merkmal Specified character. | Pruefmethode Test Method | Prue Ergebnis Test result | Spezifikation Specification |
| Gehalt ( 2-Mercaptoethanol) Assay (2 Mercaptoethanol) | GC (BASF Methode) GC (BASF Method) | 99.8 Area-% | >=99.8 |
| Wasser Water | DIN ISO 3733 DIN ISO 3733 | 0.20% | <=0.5 |
| Farbzahl [AHPA] Colour [AHPA] | DIN ISO 6271 DIN ISO 6271 | 5 | <=0.20 |
| Thiodiglykol Thiodiglycol | GC (BASF Methode) GC (BASF Method) | 0.00 Area-% | <=0.25 |
| Dithiodiglykol Dithiodiglycol | GC (BASF Methode) GC (BASF Method) | 0.00 Area-% | <=0.25 |
| Sr No | Parameters | Specifications | Results |
| 1 | Appearance | A White grey to yellow Colored Powder | A White grey to yellow Colored Powder |
| 2 | Assay by Titration | NLT 98% w/w | 99.27% |
| Item | Specifications | Result |
| Appearance | White Crystalline Powder | White Crystalline |
| Assay | 99.5% min | 99.80% |
| Melting Point | 198.5-201.5 Deg C | 200.4-201.3 |
| Clarity of water Solution | Transparency, colorless, None Suspended Matters | Pass |
| pH value of 1% aqueous solution | 5.0-7.0 | 5.91 |
| Specific Optical rotation | [a] D2c66+2 deg | -64.9 |
| Arsenic | <=2 ppm | Pass |
| Hydroquinone | <=10 ppm | Pass |
| Heavy Metal | <=10 ppm | Pass |
| Loss on drying | <=0.5% | 0.05% |
| Lgnition Residue | <=0.5% | 0.08% |
| Pathogen | Bacteria: <=300cfu/g Fungus: <=100cfu/g | <20 <20 |
| Conclasion | Pass |
| Analytical Test | Specification Limit | |||||
| Method No. | Characteristic | Lower | Upper | Value | Unit | Status |
| Addendum 00 | Pass or Fail | Pass | - | P | ||
| AT900000 | Revision Number | 1.0% | Pass | - | P | |
| ATQ30000 | Appearance (color) | Yellow To Reddish Yellow | Pass | - | P | |
| ATQ30000 | Appearance (Clarity) | Clear to Slightly Turbid | Pass | - | P | |
| ATQ30000 | Appearance (From) | Liquid | Pass | - | P | |
| ATQ32170 | Dilution (10% Aq. Solution) | Clear | Pass | - | P | |
| ATQ30160 | PH(10% Aq. Solution) | 6 | 8 | 6.7 | P | |
| ETQ30860 | Acid Value | 0 | 14 | 9.8 | mg KOH/g | P |
| ETQ30930 | SO3 Conten | 6 | 8 | 6.9 | % | P |
| Parameters | Index | Text Results |
| Appearance | White powder Crystals | White Powder Crystals |
| Identification | Qualified | Qualified |
| Melting Point Deg C | >=170 | 174.1 |
| Purity (Chemical Method)% | - | 96.6 |
| Specific Optical Rotation | -2 Deg -+5 Deg | 0.1” |
| PPM Halogens. PPM | <350 | Qualified |
| Appearance | Clear Yellow Viscous Liquid |
| Color | Y 2.2 and R 0.3 units |
| Iodine Value | 88.23 |
| F.F.A | 0.51 Oleic Acid |
| MIV | 0.09% |
| Sap Value | 179.10% |
| Unsap Value | 0.71% |
| Argemone | Negative |
| Refractive Index | 1.4716 |
| Sr No | Parameter | Observations |
| 1 | Physical Appearance | Clear Colur less Liquid |
| 2 | Odour | Pungent |
| 3 | Specific Gravity @25 deg C | 1.42 deg C + 1.48 Deg C |
| 4 | Freezing Point | - |
| 5 | Purity By GC | 99.67% |
| 6 | Boiling Range | 105 Deg C to 107 Deg C |
| Name | Clove oil (PG) |
| Description | A pale Yellow liquid becoming darker by ageing. Odour and taste those of clove |
| Solubility | Soluble in two volumes of alcohol |
| Wt/ml (at 25 deg C) | 1.0433 |
| Refractive index (at 25 Deg ) | 152.9 |
| Optical rotation | -1 Deg |
| Assay | 31.2 v/v Eugenol by GLC |
| Determination | I.P Limits | Results |
| Description | A White Crystalline Powder | Complies |
| Identification | A] When Heated it melts. Swells up and burns and and odor of burnt sugar is perceptible. B] Dissolve 0.1 g in 10 ml of water. Add 3 ml potassium cupric tartrate solutions: he solution in blue and clear. Heat to boiling. A copious red precipitate is formed | Complies |
| Appearance and odour of Solution | Dissolve 10.0 g in 15 ml of water. The solutions in clear. Not more intensely coloured than reference solution BYS7 and is odourless. | |
| Acidity or alkalinity | NMT 0.15 ml of 01 M NaOH per 6 gm of the substance. | Complies |
| Specific Optical Rotation (10% W/V Solution) | 52.50-+53.30% | 0.10% |
| Arsenic | NMT 1 ppm | 52.93 |
| Heavy Metals | NMT 5 ppm | Complies |
| Chloride | NMT 125 ppm | Complies |
| Sulphate | NMT 200 ppm | Complies |
| Sulphate | Conforms | Complies |
| Barium | Conforms | Complies |
| Foreign Sugars, Soluble Starch And dextrins | Conforms | Complies |
| Sulphated Ash | NMT 0.10% | 0.031 |
| Water | NMT 1.0% w/w | 0.47 |
| Sr. Nos Characteristics | Specifications | Result |
| Description | White Crystalline Powder Odorless, with Sweet taste. | Complies |
| Identification | A] When heated, it melts, swells up and burns And and odor of burnt sugar is perceptible B] Dissolve 0.1 g in 10 ml of water, Add 3 ml of potassium cupri-taratrate Solutions; the solution is Blue and Clear. Heat to boiling. A copious red Precipitate is formed | Complies |
| Appearance and Odour of solution | Dissolve 10.0 g in 15 ml of water. The Solution is clear. Not more intensely colour that reference solution ByS7.. and is odourless | Complies |
| Acidity or alkalinity | NMT0.15 ml of 0.1 M NaOH per 6.0 g of substance. | 0.095 |
| Specific Optical Rotation | Between +52.50 to 53.30 on dried basis | 52.97 |
| Arsenic | NMT 1 PPM | Complies |
| Heavy Metal | NMT 5 PPM | Complies |
| Chloride | NMT 125 PPM | Complies |
| Sulphate | NMT 200 PPM | Complies |
| Sulphate | Complies with the specified test as per IP 2012 | Complies |
| Barium | Complies with specified test as per IP 2012 | Complies |
| Foregin Sugars Soluble Starch and dextrin. | Complies with the specified test as per IP 2012 | Complies |
| Sulphate Ash% | NMT 0.1% | 0.039 |
| Water % | 7.0-9.5% | 7.64 |
| Lot No | Quantitiy (KGS) | Purity (Specifications: 99% min) | Loss on Drying (Specifications: 0.3% max) | Manufacturing Date | Expiry Date |
| 35E416 | 20000 | 99.40% | Meets Test | 16.May 2015 | 15. May. 2020 |
| Item | Specification | Test result |
| Description | White crystals or crystalline powder | Conforms |
| Specific rotation¿¿¿α¿¿¿D20 | +5.5° to +7.0° | +6.05° |
| State of solution | Not less than 98.0% | 99.20% |
| Chloride (Cl) | 19.89 to 20.29% | 20.03% |
| Assay | 99.0% to 100.5% | 99.50% |
| Loss on drying | 8.5 to 12.0% | 11.70% |
| Other amino acid | Chromatographically Not detectable | Conforms |
| Heavy metals (Pb) | Not more than 0.001% | < 0.001% |
| Residue on ignition | Not more than 0.1% | < 0.1% |
| Iron(Fe) | Not more than 0.001% | < 0.001% |
| Ammonium(NH4) | Not more than 0.02% | < 0.02% |
| Sulfate (SO4) | Not more than 0.020% | < 0.020% |
| PH | 1.5 to 2.0 | 1.7 |
| Arsenic(As2O3) | Not more than 0.0001% | < 0.0001% |
| Parameters | Standards | Results |
| Description | Colorless to yellowishting thick Viscous syrup, sweet in taste | Complies |
| Odor | Odorless | Complies |
| D.S.% | 85+/-1% | 85.4 |
| D.E Value % | 38-44% | 41.89 |
| PH (50% W/e) | 4.80-5.50 | 5.4 |
| Sulfur Dioxide. Ppm | 50 Max | 20.54 |
| Total Ash % | 0.50 Max | 0.012 |
| Free Starch | Bil | Complies |
| Sr. No | Parameters | Specifications | B. No |
| 2C040417 | |||
| 1 | Appearance | White to Cream Color fine fluffy Powder | Comply |
| 2 | Clarity | Clear, Limpid to slightly opalescent, without sediment | Comply |
| 3 | Moisture %w/w | 5.00 Max | 3.86 |
| 4 | pH.(10% w/v soln) | 4.50-6.50 | 5.22 |
| 5 | Dextrose Equivalent % on DB | 16.00-20.00 | 18.07 |
| 6 | Sulphated Ash% on DB | 0.50 Max | 0.03 |
| 7 | Starch Test | Negative | Comply |
| 8 | Bulk Density (packed) gm/ml | 0.28-0.45 | 0.34 |
| S. No | Parameter | Specification | Analysis |
| 1 | Appearance @25 Deg C | Waxy solid / Flakes | Complies |
| 2 | Moisture w/w(%) | 0.50 max | 0.2 |
| 3 | PH (5% aq.soin.@27 Deg C) | 6.0-7.0 | 6.7 |
| 4 | Hydroxyl Value (mgKOH/g) | 30.0-36.0 | 33.2 |
| 5 | Viscosity @100 deg C (Cst) | 76.0-100.0 | 91.85 |
| 6 | Solubility | Complete Solublity in Water | Complies |
| 7 | Congealing Point (Deg c) | 54.0-58.0 | 54 |
| 8 | Sulphated ash by wt.(%) | 0.10 Max | 0.04 |
| 9 | Arsenic (ppm) | 3.0 Max | <3.0 |
| 10 | Heavy Metal (ppm) | 5.0 max | <5.0 |
| 11 | Free EO (ppm) | 10.0 Max | <10 |
| 12 | 1.4 dioxane (PPM) | 10.0 Max | <10 |
| 13 | Acidity as acetic acid (%) | 0.05 max | 0.01 |
| 14 | Peroxide Value | Nil | Complies |
| 15 | Iodine Value | Nil | Complies |
| 16 | Aldehyde content (ppm) | 30.0 Max | <30 |
| Test | Unit | Typical |
| Appearance | -- | White Crystal Powder |
| Assay | WT% | 98.14 |
| Thiosulfate | WT% | <0.10 |
| Iron | ppm | 0.4 |
| pH | -- | 4.21 |
| Bulk Density | gm/cc | 1.174 |
| Heavy Metal as pb | ppm | 6 |
| Lead | ppm | <2.00 |
| Selenium | ppm | <1.00 |
| Potassium | -- | Pass test |
| Sulphite | -- | Pass test |
| Solubility | -- | Soluble in water, Not soluble in ethanol |
| Item | Standard | Result |
| Total Phosphates (as P2O5) | 68.0%min | 68.5 |
| Inactive Phosphates | 7.5% max | 7.2 |
| Fe (iron) Less Than | 0.03% max | 0.03 |
| PH | 5.8-7.0 | 6.1 |
| Finess: Passing through 80 mesh | 0.04 | 0.05 |
| Water Insoluble % Less Than | White powder | Pass |
| Sr No | Characteristic | Unit | Specifications Limit | Result | Test Method |
| 1 | Appearance | --- | Clear and substantially free from Suspended Matter | Test Passes | Visual |
| 2 | Acidity As Acetic Acid % | %Wt. | 0.01 Max | 0.0011 | ASTM-D1613-03 |
| 3 | Ash content | %Wt. | 0.005 Max | 0.0011 | ASTM-D482-03 |
| 4 | Color | Pt-Co | 25 Max | 15 | ASTM-D1209 |
| 5 | TEG By GC Deg By GC HG By GC | % Wt. | 99.5 Min 0.3 Max 0.2 Max | 99.92 0.06 0.01 | ASTM E-2409-04 |
| 6 | Distillation Range 760 mm Hg | ASTM D-1078-013 | |||
| Min (5%) | Deg C | 280 Min | 282 | ||
| Max (95%) | Deg C | 290 Min | 288 | ||
| 7 | Specific Gravity @20 Deg C | -- | 1.121-1.126 | 1.123 | ASTM D 891-95 |
| 8 | Water content | % Wt. | 0.1 Max | 0.031 | ASTM E 203-01 |
