Prue Merkmal Specified character. | Pruefmethode Test Method | Prue Ergebnis Test result | Spezifikation Specification |
Gehalt ( 2-Mercaptoethanol) Assay (2 Mercaptoethanol) | GC (BASF Methode) GC (BASF Method) | 99.8 Area-% | >=99.8 |
Wasser Water | DIN ISO 3733 DIN ISO 3733 | 0.20% | <=0.5 |
Farbzahl [AHPA] Colour [AHPA] | DIN ISO 6271 DIN ISO 6271 | 5 | <=0.20 |
Thiodiglykol Thiodiglycol | GC (BASF Methode) GC (BASF Method) | 0.00 Area-% | <=0.25 |
Dithiodiglykol Dithiodiglycol | GC (BASF Methode) GC (BASF Method) | 0.00 Area-% | <=0.25 |
Order No | P.O T120150713-CC |
L/C No | 560Lco1152010006 |
Commodity | Pentaery thritol |
Lot No | 150713T |
Quantity | 20000 Kg |
Characteristic | Result |
Purity | 99.00% |
Hydroxyl content | 48.90% |
Moisture Content | 0.02% |
Coloration Degree by phtalic acid resin | 1 |
Melting point in deg C beginning of melting | Min 180 |
Appearance | White Powder |
Sr No | Parameters | Specifications | Results |
1 | Appearance | A White grey to yellow Colored Powder | A White grey to yellow Colored Powder |
2 | Assay by Titration | NLT 98% w/w | 99.27% |
Appearance | Clear Yellow Viscous Liquid |
Color | Y 2.2 and R 0.3 units |
Iodine Value | 88.23 |
F.F.A | 0.51 Oleic Acid |
MIV | 0.09% |
Sap Value | 179.10% |
Unsap Value | 0.71% |
Argemone | Negative |
Refractive Index | 1.4716 |
Parameters | Standards | Results |
Description | Colorless to yellowishting thick Viscous syrup, sweet in taste | Complies |
Odor | Odorless | Complies |
D.S.% | 85+/-1% | 85.4 |
D.E Value % | 38-44% | 41.89 |
PH (50% W/e) | 4.80-5.50 | 5.4 |
Sulfur Dioxide. Ppm | 50 Max | 20.54 |
Total Ash % | 0.50 Max | 0.012 |
Free Starch | Bil | Complies |
Item | Specifications | Result |
Appearance | White Crystalline Powder | White Crystalline |
Assay | 99.5% min | 99.80% |
Melting Point | 198.5-201.5 Deg C | 200.4-201.3 |
Clarity of water Solution | Transparency, colorless, None Suspended Matters | Pass |
pH value of 1% aqueous solution | 5.0-7.0 | 5.91 |
Specific Optical rotation | [a] D2c66+2 deg | -64.9 |
Arsenic | <=2 ppm | Pass |
Hydroquinone | <=10 ppm | Pass |
Heavy Metal | <=10 ppm | Pass |
Loss on drying | <=0.5% | 0.05% |
Lgnition Residue | <=0.5% | 0.08% |
Pathogen | Bacteria: <=300cfu/g Fungus: <=100cfu/g | <20 <20 |
Conclasion | Pass |
Analytical Test | Specification Limit | |||||
Method No. | Characteristic | Lower | Upper | Value | Unit | Status |
Addendum 00 | Pass or Fail | Pass | - | P | ||
AT900000 | Revision Number | 1.0% | Pass | - | P | |
ATQ30000 | Appearance (color) | Yellow To Reddish Yellow | Pass | - | P | |
ATQ30000 | Appearance (Clarity) | Clear to Slightly Turbid | Pass | - | P | |
ATQ30000 | Appearance (From) | Liquid | Pass | - | P | |
ATQ32170 | Dilution (10% Aq. Solution) | Clear | Pass | - | P | |
ATQ30160 | PH(10% Aq. Solution) | 6 | 8 | 6.7 | P | |
ETQ30860 | Acid Value | 0 | 14 | 9.8 | mg KOH/g | P |
ETQ30930 | SO3 Conten | 6 | 8 | 6.9 | % | P |
Parameters | Index | Text Results |
Appearance | White powder Crystals | White Powder Crystals |
Identification | Qualified | Qualified |
Melting Point Deg C | >=170 | 174.1 |
Purity (Chemical Method)% | - | 96.6 |
Specific Optical Rotation | -2 Deg -+5 Deg | 0.1” |
PPM Halogens. PPM | <350 | Qualified |
Sr No | Parameter | Observations |
1 | Physical Appearance | Clear Colur less Liquid |
2 | Odour | Pungent |
3 | Specific Gravity @25 deg C | 1.42 deg C + 1.48 Deg C |
4 | Freezing Point | - |
5 | Purity By GC | 99.67% |
6 | Boiling Range | 105 Deg C to 107 Deg C |
Name | Clove oil (PG) |
Description | A pale Yellow liquid becoming darker by ageing. Odour and taste those of clove |
Solubility | Soluble in two volumes of alcohol |
Wt/ml (at 25 deg C) | 1.0433 |
Refractive index (at 25 Deg ) | 152.9 |
Optical rotation | -1 Deg |
Assay | 31.2 v/v Eugenol by GLC |
Determination | I.P Limits | Results |
Description | A White Crystalline Powder | Complies |
Identification | A] When Heated it melts. Swells up and burns and and odor of burnt sugar is perceptible. B] Dissolve 0.1 g in 10 ml of water. Add 3 ml potassium cupric tartrate solutions: he solution in blue and clear. Heat to boiling. A copious red precipitate is formed | Complies |
Appearance and odour of Solution | Dissolve 10.0 g in 15 ml of water. The solutions in clear. Not more intensely coloured than reference solution BYS7 and is odourless. | |
Acidity or alkalinity | NMT 0.15 ml of 01 M NaOH per 6 gm of the substance. | Complies |
Specific Optical Rotation (10% W/V Solution) | 52.50-+53.30% | 0.10% |
Arsenic | NMT 1 ppm | 52.93 |
Heavy Metals | NMT 5 ppm | Complies |
Chloride | NMT 125 ppm | Complies |
Sulphate | NMT 200 ppm | Complies |
Sulphate | Conforms | Complies |
Barium | Conforms | Complies |
Foreign Sugars, Soluble Starch And dextrins | Conforms | Complies |
Sulphated Ash | NMT 0.10% | 0.031 |
Water | NMT 1.0% w/w | 0.47 |
Sr. Nos Characteristics | Specifications | Result |
Description | White Crystalline Powder Odorless, with Sweet taste. | Complies |
Identification | A] When heated, it melts, swells up and burns And and odor of burnt sugar is perceptible B] Dissolve 0.1 g in 10 ml of water, Add 3 ml of potassium cupri-taratrate Solutions; the solution is Blue and Clear. Heat to boiling. A copious red Precipitate is formed | Complies |
Appearance and Odour of solution | Dissolve 10.0 g in 15 ml of water. The Solution is clear. Not more intensely colour that reference solution ByS7.. and is odourless | Complies |
Acidity or alkalinity | NMT0.15 ml of 0.1 M NaOH per 6.0 g of substance. | 0.095 |
Specific Optical Rotation | Between +52.50 to 53.30 on dried basis | 52.97 |
Arsenic | NMT 1 PPM | Complies |
Heavy Metal | NMT 5 PPM | Complies |
Chloride | NMT 125 PPM | Complies |
Sulphate | NMT 200 PPM | Complies |
Sulphate | Complies with the specified test as per IP 2012 | Complies |
Barium | Complies with specified test as per IP 2012 | Complies |
Foregin Sugars Soluble Starch and dextrin. | Complies with the specified test as per IP 2012 | Complies |
Sulphate Ash% | NMT 0.1% | 0.039 |
Water % | 7.0-9.5% | 7.64 |
Lot No | Quantitiy (KGS) | Purity (Specifications: 99% min) | Loss on Drying (Specifications: 0.3% max) | Manufacturing Date | Expiry Date |
35E416 | 20000 | 99.40% | Meets Test | 16.May 2015 | 15. May. 2020 |
Item | Specification | Test result |
Description | White crystals or crystalline powder | Conforms |
Specific rotation¿¿¿α¿¿¿D20 | +5.5° to +7.0° | +6.05° |
State of solution | Not less than 98.0% | 99.20% |
Chloride (Cl) | 19.89 to 20.29% | 20.03% |
Assay | 99.0% to 100.5% | 99.50% |
Loss on drying | 8.5 to 12.0% | 11.70% |
Other amino acid | Chromatographically Not detectable | Conforms |
Heavy metals (Pb) | Not more than 0.001% | < 0.001% |
Residue on ignition | Not more than 0.1% | < 0.1% |
Iron(Fe) | Not more than 0.001% | < 0.001% |
Ammonium(NH4) | Not more than 0.02% | < 0.02% |
Sulfate (SO4) | Not more than 0.020% | < 0.020% |
PH | 1.5 to 2.0 | 1.7 |
Arsenic(As2O3) | Not more than 0.0001% | < 0.0001% |
Sr. No | Parameters | Specifications | B. No |
2C040417 | |||
1 | Appearance | White to Cream Color fine fluffy Powder | Comply |
2 | Clarity | Clear, Limpid to slightly opalescent, without sediment | Comply |
3 | Moisture %w/w | 5.00 Max | 3.86 |
4 | pH.(10% w/v soln) | 4.50-6.50 | 5.22 |
5 | Dextrose Equivalent % on DB | 16.00-20.00 | 18.07 |
6 | Sulphated Ash% on DB | 0.50 Max | 0.03 |
7 | Starch Test | Negative | Comply |
8 | Bulk Density (packed) gm/ml | 0.28-0.45 | 0.34 |
S. No | Parameter | Specification | Analysis |
1 | Appearance @25 Deg C | Waxy solid / Flakes | Complies |
2 | Moisture w/w(%) | 0.50 max | 0.2 |
3 | PH (5% aq.soin.@27 Deg C) | 6.0-7.0 | 6.7 |
4 | Hydroxyl Value (mgKOH/g) | 30.0-36.0 | 33.2 |
5 | Viscosity @100 deg C (Cst) | 76.0-100.0 | 91.85 |
6 | Solubility | Complete Solublity in Water | Complies |
7 | Congealing Point (Deg c) | 54.0-58.0 | 54 |
8 | Sulphated ash by wt.(%) | 0.10 Max | 0.04 |
9 | Arsenic (ppm) | 3.0 Max | <3.0 |
10 | Heavy Metal (ppm) | 5.0 max | <5.0 |
11 | Free EO (ppm) | 10.0 Max | <10 |
12 | 1.4 dioxane (PPM) | 10.0 Max | <10 |
13 | Acidity as acetic acid (%) | 0.05 max | 0.01 |
14 | Peroxide Value | Nil | Complies |
15 | Iodine Value | Nil | Complies |
16 | Aldehyde content (ppm) | 30.0 Max | <30 |
Test | Unit | Typical |
Appearance | -- | White Crystal Powder |
Assay | WT% | 98.14 |
Thiosulfate | WT% | <0.10 |
Iron | ppm | 0.4 |
pH | -- | 4.21 |
Bulk Density | gm/cc | 1.174 |
Heavy Metal as pb | ppm | 6 |
Lead | ppm | <2.00 |
Selenium | ppm | <1.00 |
Potassium | -- | Pass test |
Sulphite | -- | Pass test |
Solubility | -- | Soluble in water, Not soluble in ethanol |
Item | Standard | Result |
Total Phosphates (as P2O5) | 68.0%min | 68.5 |
Inactive Phosphates | 7.5% max | 7.2 |
Fe (iron) Less Than | 0.03% max | 0.03 |
PH | 5.8-7.0 | 6.1 |
Finess: Passing through 80 mesh | 0.04 | 0.05 |
Water Insoluble % Less Than | White powder | Pass |
Sr No | Characteristic | Unit | Specifications Limit | Result | Test Method |
1 | Appearance | --- | Clear and substantially free from Suspended Matter | Test Passes | Visual |
2 | Acidity As Acetic Acid % | %Wt. | 0.01 Max | 0.0011 | ASTM-D1613-03 |
3 | Ash content | %Wt. | 0.005 Max | 0.0011 | ASTM-D482-03 |
4 | Color | Pt-Co | 25 Max | 15 | ASTM-D1209 |
5 | TEG By GC Deg By GC HG By GC | % Wt. | 99.5 Min 0.3 Max 0.2 Max | 99.92 0.06 0.01 | ASTM E-2409-04 |
6 | Distillation Range 760 mm Hg | ASTM D-1078-013 | |||
Min (5%) | Deg C | 280 Min | 282 | ||
Max (95%) | Deg C | 290 Min | 288 | ||
7 | Specific Gravity @20 Deg C | -- | 1.121-1.126 | 1.123 | ASTM D 891-95 |
8 | Water content | % Wt. | 0.1 Max | 0.031 | ASTM E 203-01 |
3.3/5
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